Mechanical performance of lime kiln dust, silica fume, and recycled carpet fiber mixtures for clay stabilization compared to cement under freeze-thaw cycles

Document Type : Research Paper

Authors

1 Department of Civil Engineering, CT.C., Islamic Azad University, Tehran, Iran.

2 Department of Mining Engineering, Amirkabir University of technology, Tehran, Iran.

10.22124/jcr.2026.33714.1741

Abstract

Due to the high energy consumption and carbon emissions associated with cement production, finding alternative mixtures with mechanical performance comparable or superior to that of cement under harsh environmental conditions such as freeze-thaw cycles has become a necessity. This study investigates the mechanical performance of mixtures containing industrial wastes, including lime kiln dust, silica fume, and waste carpet fibers, in comparison with a cement sample under freeze-thaw cycle conditions. The main objective is to achieve a stable and durable mixture with suitable replaceability for cement in geotechnical applications in cold regions. For this purpose, the effects of lime kiln dust (up to 10%), silica fume (up to 100% as a replacement for lime kiln dust), and carpet fibers (up to 2%), along with cement-containing mixtures (up to 10% cement), were evaluated. The results indicated that the optimal mixture, consisting of 5% lime kiln dust, 50% silica fume, and 1% carpet fibers, achieved a compressive strength exceeding 7000 kPa and a tensile strength of 600 kPa, demonstrating significantly superior performance compared to the reference cement sample. After 8 freeze-thaw cycles, this mixture retained over 97% of its initial strength, indicating its superior resistance compared to the cement sample under successive freeze-thaw conditions. Carpet fibers, by providing bridging across microcracks, significantly enhanced the tensile strength of this mixture. Overall, the introduced optimal mixture exhibits considerable superiority in terms of mechanical performance and durability compared to the cement sample and can be considered an environmentally friendly and efficient alternative.

Keywords


[1] A. Zerrouk, B. Lamri, C. Vipulanandan, S. Kenai, Performance evaluation of human hair fiber reinforcement on lime or cement stabilized clayey-sand, in: Key Eng. Mater., Trans Tech Publ, 2016: pp. 207–217.
[2] A. Ghorbani, M. Salimzadehshooiili, Evaluation of Strength behaviour of Cement-RHA Stabilized and Polypropylene Fiber Reinforced Clay-Sand Mixtures, Civil Engineering Journal 4 (2018) 2628–2641.
[3] H.C. Scheuermann Filho, R. Beck Saldanha, C. Gravina da Rocha, N. Cesar Consoli, Sustainable Binders Stabilizing Dispersive Clay, Journal of Materials in Civil Engineering 33 (2021) 06020026. https://doi.org/10.1061/(asce)mt.1943-5533.0003595.
[4] N. Latifi, A.S.A. Rashid, S. Siddiqua, S. Horpibulsuk, Micro-structural analysis of strength development in low-and high swelling clays stabilized with magnesium chloride solution—A green soil stabilizer, Appl. Clay Sci. 118 (2015) 195–206.
[5] R.N. Yong, V.R. Ouhadi, Experimental study on instability of bases on natural and lime/cement-stabilized clayey soils, Appl. Clay Sci. 35 (2007) 238–249. https://doi.org/10.1016/j.clay.2006.08.009.
[6] R. Mahmoudi, R. Rezvani, I. Hosseinpour, M. Payan, A. Ghanbari Astaneh, Effects of Hydrated Lime and Zeolite on the Mechanical Behavior of Calcareous Sand Subjected to Wet–Dry Cycles, Journal of Materials in Civil Engineering 37 (2025) 04024478. https://doi.org/10.1061/JMCEE7.MTENG-17997.
[7] D.-L. Wang, C.-S. Tang, X.-H. Pan, Z.-H. Dong, R. Wang, J.-Z. Zhang, X.-L. Ji, H.-C. Hu, B. Shi, Construction and Demolition Waste Stabilization through Biocarbonation of Reactive Magnesia Cement: Effect of Urea Concentration, Journal of Materials in Civil Engineering 37 (2025) 04024450. https://doi.org/10.1061/JMCEE7.MTENG-17257.
[8] M. Ramezani, S. Soleimani Kutanaei, A. Seyedkazemi, A. Esfandiari Fard, Sustainable stabilization of fiber-reinforced clayey sand using zeolite as partial cement replacement, Case Studies in Construction Materials 22 (2025) e04868. https://doi.org/10.1016/j.cscm.2025.e04868.
[9] A. Khajeh, M. Salimi, H. MolaAbasi, M.E. Seif, M. Payan, S. Keawsawasvong, Zeolite-based soil stabilization: A review, Journal of Rock Mechanics and Geotechnical Engineering (2025). https://doi.org/10.1016/j.jrmge.2025.06.039.
[10] M. Dokaneh, M. Salimi, R. Rezvani, M. Payan, I. Hosseinpour, Valorization of industrial wastes for stabilizing highly expansive clays: Mechanical, microstructural and durability improvements, Constr. Build. Mater. 481 (2025) 141497. https://doi.org/10.1016/j.conbuildmat.2025.141497
[11] M. Salimi, M. Payan, I. Hosseinpour, M. Arabani, P. Zanganeh Ranjbar, Geopolymer stabilization of construction and demolition waste using water treatment sludge and silica fume for pavement applications, Journal of Materials Research and Technology 37 (2025) 1834–1849. https://doi.org/10.1016/j.jmrt.2025.06.096.
[12] A. Mohammadi Darestani, M. Arabani, P. Zanganeh Ranjbar, M. Payan, M. Salimi, Strength enhancement of calcium carbide residue-stabilized clay with perlite powder and water treatment sludge, Sci. Rep. 15 (2025) 43701. https://doi.org/10.1038/s41598-025-27584-8.
[13] A. Jamaldar, P. Asadi, M. Salimi, M. Payan, P.Z. Ranjbar, M. Arabani, H. Ahmadi, Application of natural and synthetic fibers in bio-based earthen composites: A state-of-the-art review, Results in Engineering 25 (2025) 103732. https://doi.org/10.1016/j.rineng.2024.103732.
[14] M.H. Hatefi, M. Arabani, M. Payan, P. Zanganeh Ranjbar, The influence of volcanic ash (VA) on the mechanical properties and freeze-thaw durability of lime kiln dust (LKD)-stabilized kaolin clayey soil, Results in Engineering 24 (2024) 103077. https://doi.org/10.1016/j.rineng.2024.103077.
[15] M. Salimi, M. Payan, I. Hosseinpour, M. Arabani, P.Z. Ranjbar, Impact of clay nano-material and glass fiber on the efficacy of traditional soil stabilization technique, Mater. Lett. 360 (2024) 136046. https://doi.org/10.1016/j.matlet.2024.136046.
[16] P. Zanganeh Ranjbar, H. Talebi Mamoudan, R. Mousazadeh Moghadampour, M. Ghorbani, Investigating the synergistic effect of using cement, polymer slurry, and recycled tire fibers in improving the mechanical and geotechnical properties of dune sand, Concrete Research 15 (2022) 31–43.
[17] M.H. Hosseinjani Miyandehi, P. Zanganeh Ranjbar, M.A. Lashteh Neshaei, M.M. Ranjbar Taklymie, H. Nassiraei, Investigation of Alkaline Reaction of Dredged Caspian Sea Marine Sand to Make Concrete in Marine Environment and Ports, Concrete Research 15 (2022) 5–22.
[18] P. Zanganeh Ranjbar, M. Sohrabi Guilani, A. Salehi, M. Ghasemi Laskoukalayeh, Evaluation of porous concrete containing waste-originated activated carbon in the removal of surface runoff pollutants, Concrete Research 16 (2024) 49–63.
[19] S.A.M. Moayed, M. Arabani, H. Ahmadi, Influence of hemp fiber on the mechanical characteristics and freeze-thaw durability of LKD-nano silica-stabilized kaolin soil, Results in Engineering 26 (2025) 105318. https://doi.org/10.1016/j.rineng.2025.105318.
[20] M. Hematibahar, N. Vatin, J. Petrů, M.N. Bashir, A. Hasanzadeh, T. Gebre, A.A. Milani, A. Bakhtiyari, Experimental evaluation of mechanical strength of silica fume-cemented sand reinforced with 3D-printed fibers, Journal of Materials Research and Technology 38 (2025) 2058–2075. https://doi.org/10.1016/j.jmrt.2025.08.041.
[21] M. Waleed, F. Alshawmar, Enhancing mechanical properties of low plasticity soil through coal and silica fume stabilization, Sci. Rep. 15 (2025) 1–22. https://doi.org/10.1038/s41598-025-94149-0.
[22] A. Hasanzadeh, I. Shooshpasha, Influence of PET fibres on the tensile characteristics of cemented sand treated with silica fume, Road Materials and Pavement Design 26 (2025) 1041–1064. https://doi.org/10.1080/14680629.2024.2399251.
[23] J.F. Zhu, Q.Q. Zheng, Y.L. Tao, L.Y. Ju, H. Yang, X.N. Gong, B.J. Pan, Z.Q. Wang, The curing mechanism and empirical model for the marine organic soft clay stabilized with calcium carbide residue and silica fume under the optimal ratio, Acta Geotech. 20 (2025) 683–706. https://doi.org/10.1007/s11440-024-02413-w.
[24] H. Ghiassian, R. Jamshidi, A.R. Tabarsa, Dynamic performance of Toyoura sand reinforced with randomly distributed carpet waste strips, in: Geotechnical Earthquake Engineering and Soil Dynamics IV, 2008: pp. 1–13.
[25] M. Miraftab, A. Lickfold, Utilization of Carpet Waste in Reinforcement of Substandard Soils, Journal of Industrial Textiles 38 (2008) 167–174. https://doi.org/10.1177/1528083708091064.
[26] M. Mirzababaei, M. Miraftab, M. Mohamed, P. McMahon, Unconfined Compression Strength of Reinforced Clays with Carpet Waste Fibers, Journal of Geotechnical and Geoenvironmental Engineering 139 (2013) 483–493. https://doi.org/10.1061/(ASCE)GT.1943-5606.0000792.
[27] M. Shahbazi, M. Rowshanzamir, S.M. Abtahi, S.M. Hejazi, Optimization of carpet waste fibers and steel slag particles to reinforce expansive soil using response surface methodology, Appl. Clay Sci. 142 (2017) 185–192. https://doi.org/10.1016/j.clay.2016.11.027.
[28] A.R. Goodarzi, H.R. Akbari, M. Salimi, Enhanced stabilization of highly expansive clays by mixing cement and silica fume, Appl. Clay Sci. 132–133 (2016) 675–684. https://doi.org/10.1016/j.clay.2016.08.023.
[29] B. Uzal, L. Turanl, H.N. Yücel, M.C. Göncüoğlu, A. Çulfaz, Pozzolanic activity of clinoptilolite: a comparative study with silica fume, fly ash and a non-zeolitic natural pozzolan, Cem. Concr. Res. 40 (2010) 398–404.
[30] M. Panigrahi, P. Biswal, N. Patel, R.I. Ganguly, R.R. Dash, Pond Ash (PA)–Jute Fiber‐Based Geopolymer Cementitious Materials, in: Development of Geopolymer from Pond Ash‐Thermal Power Plant Waste, Wiley, 2023: pp. 169–194. https://doi.org/10.1002/9781394167975.ch6.
[31] E. Kalkan, Preparation of scrap tire rubber fiber-silica fume mixtures for modification of clayey soils, Appl. Clay Sci. 80–81 (2013) 117–125. https://doi.org/10.1016/j.clay.2013.06.014.
[32] O. Plé, T.N.H. Lê, Effect of polypropylene fiber-reinforcement on the mechanical behavior of silty clay, Geotextiles and Geomembranes 32 (2012) 111–116. https://doi.org/10.1016/j.geotexmem.2011.11.004.
[33] J. Ganiev, S. Yamada, M. Nakano, T. Sakai, Effect of fiber-reinforcement on the mechanical behavior of sand approaching the critical state, Journal of Rock Mechanics and Geotechnical Engineering 14 (2022) 1241–1252. https://doi.org/10.1016/j.jrmge.2021.10.003.
[34] N.C. Consoli, L. Festugato, H.C.S. Filho, G.D. Miguel, A.T. Neto, D. Andreghetto, Durability Assessment of Soil-Pozzolan-Lime Blends through Ultrasonic-Pulse Velocity Test, Journal of Materials in Civil Engineering 32 (2020) 4020223.
[35] S.A. Abo-Qudais, Effect of concrete mixing parameters on propagation of ultrasonic waves, Constr. Build. Mater. 19 (2005) 257–263. https://doi.org/10.1016/j.conbuildmat.2004.07.022.
[36] A. Janalizadeh Choobbasti, F. Farrokhzad, A. Nadimi, S. Soleimani Kutanaei, Effects of copper sludge on cemented clay using ultrasonic pulse velocity, J. Adhes. Sci. Technol. 33 (2019) 433–444. https://doi.org/10.1080/01694243.2018.1471842.
[37] A. Hasanzadeh, I. Shooshpasha, Influences of silica fume particles and polyethylene terephthalate fibers on the mechanical characteristics of cement-treated sandy soil using ultrasonic pulse velocity, Bulletin of Engineering Geology and the Environment 81 (2022) 1–17. https://doi.org/10.1007/s10064-021-02494-x.